Asian Journal of Research in Chemistry

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Green Synthesis of Nitrone and Isoxazolidines:A Convenient Method of Synthesis in Water


Affiliations
1 Organic Chemistry Laboratory, Sikkim Government College, Gangtok, Sikkim 737102, India
     

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Novel C,N-diphenyl--amino nitrone has been synthesized in water and 1,3 dipolar cycloaddition reaction of the nitrone has been studied with maleimides in water. Significant rate acceleration and high yield of these reactions are observed in water compared with organic solvents. The structures of all the compounds have been established on the basis of spectral and analytical data.


Keywords

C, N-Diphenyl-α-Amino Nitrone, Cycloaddition Reaction, Aqueous Phase.
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  • Green Synthesis of Nitrone and Isoxazolidines:A Convenient Method of Synthesis in Water

Abstract Views: 314  |  PDF Views: 1

Authors

Bhaskar Chakraborty
Organic Chemistry Laboratory, Sikkim Government College, Gangtok, Sikkim 737102, India
Neelam Rai
Organic Chemistry Laboratory, Sikkim Government College, Gangtok, Sikkim 737102, India
Manjit S. Chhetri
Organic Chemistry Laboratory, Sikkim Government College, Gangtok, Sikkim 737102, India
Prawin K. Sharma
Organic Chemistry Laboratory, Sikkim Government College, Gangtok, Sikkim 737102, India

Abstract


Novel C,N-diphenyl--amino nitrone has been synthesized in water and 1,3 dipolar cycloaddition reaction of the nitrone has been studied with maleimides in water. Significant rate acceleration and high yield of these reactions are observed in water compared with organic solvents. The structures of all the compounds have been established on the basis of spectral and analytical data.


Keywords


C, N-Diphenyl-α-Amino Nitrone, Cycloaddition Reaction, Aqueous Phase.